Optimization of nuclear magnetic resonance and gas chromatography-mass spectrometry-based fingerprinting methods to characterize goat milk powder

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چکیده

This study is the first to provide a comprehensive characterization of liquid and volatile fractions whole goat milk powder (GMP). Robust nuclear magnetic resonance (NMR)- gas chromatography-mass spectrometry (GC-MS)-based chemical fingerprinting methods were optimized implemented. The untargeted 1H-NMR analysis resolved 44 metabolites in GMP. NMR technique effectively identified coming from aliphatic, sugar, aromatic regions that can be important defining technological properties quality headspace was able detect total 50 volatiles including alkanes, ketones, alcohols, aromatics, alkenes, aldehydes, esters, acid, sulfur compounds. GMP dominated by alkane group, while only few esters detected. Goat premium product vulnerable fraudulent activities such as adulteration or counterfeit. Therefore, proper identification crucial step verify its authenticity quality.

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ژورنال

عنوان ژورنال: Journal of Dairy Science

سال: 2021

ISSN: ['0022-0302', '1525-3198', '1529-9066']

DOI: https://doi.org/10.3168/jds.2020-18467